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固相萃取法
    Methods:By using solid phase extraction and gas chromatography/mass spectroscope(GC-MS) ,main Phthalate esters in surface water samples from the urban rivers and ponds in suburb were determined.
    方法:采集市区河水和市郊鱼塘水,固相萃取法富集水样,气-质联机(GC-MS)测定水样中PAEs浓度。
    There were three main techniques of extraction and cleaning , such as liquid-liquid extraction(LLE), solid phase extraction(SPE) and supercritical fluid extraction(SFE).
    常见鸦片类毒品在体内的代谢; 生物样品中常见鸦片类毒品的提取净化方法,如液—液萃取法(LLE)、固相萃取法(SPE)和超临界流体萃取(SFE)等;
    Presently, there are many methods applied for the pretreatment of the analyzing sample extracted from plant materials such as Liquid-liquid Extraction (LLE), Simultaneous Distillation/Extraction (SDE), Supercritical Fluid Extraction (SFE) and Solid Phase Extraction (SPE), etc. but all of those mentioned above are complicated, time/labor consumptive and need large amount of plant materials.
    目前,用于植物体中挥发油类成分分析样品预处理方法很多,如液液萃取法(Liquid-liquid Extraction,LLE)、同时蒸馏萃取法(Simultaneous Distillation/Extraction,SDE)、超临界流体萃取法(Supercritical Fluid Extraction,SFE)和固相萃取法(Solid Phase Extraction,SPE)等,但都不同程度存在操作繁琐、费时费力、精确度较差等弊端;
    In solid phase extraction, extraction yield of CL is 91.25% and extraction yield of SA is 86.10% by Amberlite XAD-2 resin.
    固相萃取法中,采用Amberlite XAD-2大孔吸附树脂,效果较液-液萃取更好,萃取率为91.25%和86.10%。
    METHODS Plasma samples were pretreated by solid phase extraction. Cefpodoxime and cefuroxime (internal standard) were separated on M N Necleosil 100 5 C 18 column( 150 mm × 4.6 mm , 5 μm )at 39 ℃ with 0.05 mol ·L -1 acetate buffer of pH 3.8 methanol(82∶18)as mobile phase at a flow rate of 1 mL ·min -1 , and monitored at 234 nm .
    方法 :采用固相萃取法预处理血浆样品 ,分析柱为M N Necleosil 10 0 5C18柱 (15 0mm× 4 .6mm ,5 μm) ,流动相为pH 3.8的 0 .0 5mol·L-1醋酸缓冲液 甲醇 (82∶18) ,流速为 1mL·min-1,检测波长为 2 34nm ,柱温为 39℃ ,按内标法定量。
    A C18column was usesd with the mobile phase of methanol-water-triethylamine- acetic acid (600∶400∶ 4∶2) at the detectionwavelength of 254nm. The blood was extracted with solid phase extraction, using diazepam as internal standard.
    采用C18柱,流动相为甲醇-水-三乙胺-乙酸(600∶400∶4∶2),检测波长254nm,固相萃取法处理血样,地西泮为内标。
    Plasma samples of 18 male volunteers after oral administration of 750 mg baicalin test capsules and reference tablets were prepared by solid phase extraction and the concentrations of baicalin were determined by HPLC-UV method.
    方法:18名健康志愿者随机单剂量交叉口服黄芩苷试验胶囊和参比片750mg,血浆样品采用固相萃取法处理后,进行HPLC-UV测定。
    This method is with in the solid phase extraction method extract water and the waste water multi-fungi spirit,after takes the concentration purification to be organic directly enters the type to the highly effective liquid phase color spectrometer,examines with the diode matrix detector,according to retention time external standard law quota.
    本方法是用固相萃取法萃取水和废水中的多菌灵,取浓缩纯化后的有机相直接进样到高效液相色谱仪,用二极管矩阵检测器检测,根据保留时间外标法定量。
    The prospects of applying solid phase extraction to the analysis of traditional Chinese medicine and discussing the strategy and procedure of developing a new SPE method
    固相萃取法在中药分析中的应用前景及其建立优化新方法的策略与步骤
    Analysis of chlorothalonil and pyrethroid pesticides in water using a solid phase extraction technique
    固相萃取法测定水中百菌清和拟除虫菊酯
    Investigation on Improving the Sensitivity of Retinoic Acids by Capillary Electrophoresis and Micro-column Solid Phase Extraction
    提高维甲酸毛细管电泳分析灵敏度的微柱固相萃取法研究
    Determination of Organochlorine Pesticide Residues in Poria cocos by Ultrasonic and Solid Phase Extraction
    超声波及固相萃取法检测茯苓中有机氯农药残留
    To Detect the Organic Phosphorus Pesticide Residue in Food with Fast Solid Phase Extraction
    快速固相萃取法测定食品中多种有机磷农药残留
    Solid Phase Extraction of Hg(Ⅱ)-SBDTR Chelate with C_(18) Disks and Its Application for Determination of Mercury in Food and Water
    用对磺酸苯亚甲基硫代若丹宁固相萃取法测定食品和水中的微量汞
    Solid Phase Extraction Determination of Imidacloprid Residues in Honeysuckle
    固相萃取法测定金银花中吡虫啉的残留量
    Solid phase extraction was used to extract the organic pollutants of source water and drinking water from 5 waterworks in urban area of Chongqing in three different water phases (spring, summer, winter).
    本研究用固相萃取法提取重庆市主城区5个水厂三个不同水期(春季-平水期、夏季-丰水期、冬季-枯水期)的水源水与出厂水中有机污染物;
    In Chapter One, the basal mode, principle, methodology, applications and prospects of the solid phase extraction technique are reviewed.
    第一章:文献综述。 介绍了固相萃取法的基本模式、原理,操作方法,应用和发展前景。
    Firstly, the quantitative analysis of indoor Volatile Organic Compounds (VOCs) was done using the improved SPME device combined with GC-MS equipped with a capillary column. After optimization of the experimental conditions, The abundance of ionic apex detected in injecting sampling directly method is markedly less than that in solid phase extraction (SPE) or that in SPME measurement.
    本论文用自制的SPME与GC-MS(毛细管柱)联用,对一预处理实验室室内空气中的挥发性有机化合物进行了定性检测,优化了实验条件,同传统的直接进样法和固相萃取法(SPE)进行了对照实验,研究结果表明,直接进样法的离子峰强度明显低于固相萃取和SPME法。
    Solid phase extraction (SPE) is a sample preparation technique that originated in the 1970s and developed from the late of the 1980s, and has the advantage of high pre-concentration factor, simplicity of operation, less pollution to the environment, easy automation, and can be applied to the different samples.
    固相萃取法(SPE)是一种70年代中期出现,80年代后期才真正发展起来的试样预处理技术,与传统液-液萃取法相比,因具有富集倍数高,适用于不同体积试样,可封闭操作而避免引入污染物,吸附剂可再生使用及易于实现分离过程的在线/自动化等优点,越来越受到人们的重视,并得到广泛的应用。
    Solid phase extraction with polystyrene as stationary phase, ethanol as mobile phase was studied. The effects of onion serous Ph, activation and capacity of the extracting column, the volume of mobile phase were investigated.
    以聚苯乙烯纤维丝为固定相,乙醇为流动相,采用固相萃取法提取洋葱油,考察了洋葱浆液的Ph值、固相萃取柱的活化、固相萃取柱的柱容量以及洗脱液的体积等因素对萃取效果的影响,最佳的萃取条件为:将新鲜洋葱去皮、去根、洗净、切块后加入适量重蒸水进行匀浆(11800r/min)。
 

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