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标准
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  ' the standard '
     The implementation of "Student Physical Endowment Health Standard "(to be shortened as 'the Standard'in the following) is an important measure directed by the ideology of "Health First" for middle schools. The essay tries to analyze the problems occurred in the performance of the testing parameter according to the Standard in the middle schools and puts forward some pieces of advices.
     《学生体质健康标准》(以下简称《标准》)的实施是学校体育贯彻"健康第一"指导思想的一项重要举措,本 文对《标准》测试指标在中学实施出现的问题等进行了分析并提出建议。
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  “《标准》”译为未确定词的双语例句
     Briefly introduced the content of the national code for "Basic Terms and General Symbols used in Building and Civil Engineering Structural Design" (GBJ 132-90), the existing problems and the relations between this code and the current national code for "General Symbols, SI units and Basic Terms used in Building Structural Besign" (GBJ 83-85) are presented.
     扼要介绍国家标准《工程结构设计基本术语和通用符号》(GBJ 132-90)的内容,并阐明该《标准》与现行国家标准《建筑结构设计通用符号、计量单位和基本术语》(GBJ 83-85)的关系与存在问题。
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     In 2004, National Education Bureau issued SETC: Standards of Educational Technology of China, in which new standards of modern educational technology was presented to the staff of elementary education.
     教育部于2004年颁布了《中小学教师教育技术能力标准(SETC:Standards of Educational Technologyof China)》(简称《标准》),对基础教育的从业人员的现代教育技术水平提出了新的要求。
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     New Standard New Textbook New Target
     新《标准》 新教材 新目标
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     "ordinary high school mathematics curriculum standard (experimental)"(2003.4) (hereinafter referred to as the "standard") contains "algorithms preliminary", it's in the curriculum of five modules in mathematics 3, algorithm becomes new additions to the curriculum.
     《普通高中数学课程标准(实验)》(2003.4)(以下简称《标准》)把“算法初步”列入了必修课程的5个模块中的数学3,算法成为课程中新增加的内容。
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     Compared with the content in Mathematics Teaching Syllabus, the geometry section in Senior Middle School Mathematics Curriculum Standards has changed a lot in content structure, difficulty and requirements.
     《普通高中数学课程标准(实验)》(以下简称《标准》)与《全日制普通高级中学数学教学大纲(供实验用)》(以下简称《大纲》)中几何部分的内容设置相比,在内容结构、内容要求、内容难度等三个方面均发生了大的变化。
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     标准
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     Opportunity of Standard
     “标准”战争
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  ' the standard '
The method applies to the standard arithmetic subgroups ofSO(n,1) (a case which was proved previously by Millson [Mi]), to the non-arithmetic lattices inSO(n,1) constructed by Gromov and Piatetski-Shapiro [GPS] and to groups generated by reflections.
      
Fr?nsdal [Fr1, Fr2] made a penetrating observation that both of them are quasi-Hopf algebras, obtained by twisting the standard quantum affine algebraUq(g).
      
In addition to the standard cohomological tools in algebraic geometry, the proof crucially relies on the nonvanishing of certain 3j-symbols from the quantum theory of
      
This does not, however, give rise to vanishing identities for the standard nonsymmetric Macdonald and Koornwinder polynomials; we discuss the required modification to these polynomials to support such results.
      
Let ? denote the standard (i.e., Levi-Civita) Laplacian for some non-compact, connected, complete, separable Riemannian manifild M.
      
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The absorption band of water vapor at 0.94 μ is studied photographically by means of a concave grating spectrometer. Twenty eight component lines are observed and measured on a comparator as well as on a Moll microphotometer. This band shows something of a doublet form which suggests that the H2O molecule has a triangular form with the oxygen atom at the vertex of an obtuse angle. The lines agree closely with some of the absorption lines in the solar spectrum as measured by Abney in 1880.

前之研究红外光谱者类多依赖热电堆以测定光谱内光能之分布。吾人咸知红外带状光谱之接近可见部分者,其成分线排列甚密。若用热电堆万难分析而得其细微组织。作者所考察之光谱正在红外照相片感光范围之内,故得测定水汽带状光谱内各成分线之波长而具有1内之准确度。 作者所用分光仪器为一凹面光栅,其曲度半径为2公尺。该光栅面上每厘米划有线6000根,颇适合红外光谱之探讨。所用光源为一1000流明之电灯泡泡内有一一字形线圈灯丝,其所发之光穿过2公尺之105°—110℃水汽而交聚在分光仪之缝上。红外照相片经氨溶液之超度敏化后,即安置於已经配准之相片匣内,而使之感光。光之可见部分系用深红滤片割除。照光时间约 费四五十小时,然后除去滤片,照以水银光谱凡数秒,作为决定波长之标准。 用前法所摄得之光谱大都不十分清晰,其主要原因系由水汽管之太短。但用显微光度计量之,各成分线之波长不难准至1(?)范围以内。本实验所得各线若与五十年前Abney所测定太阳光谱中0.94μ附近之吸收线相比较,可见太阳红外光谱中许多吸收线系由大气中水汽所产生,而证实Abney最初之推想。惟本实验所测定之吸收线与Abney所测定太阳光谱中之对应黑线具有一等差...

前之研究红外光谱者类多依赖热电堆以测定光谱内光能之分布。吾人咸知红外带状光谱之接近可见部分者,其成分线排列甚密。若用热电堆万难分析而得其细微组织。作者所考察之光谱正在红外照相片感光范围之内,故得测定水汽带状光谱内各成分线之波长而具有1内之准确度。 作者所用分光仪器为一凹面光栅,其曲度半径为2公尺。该光栅面上每厘米划有线6000根,颇适合红外光谱之探讨。所用光源为一1000流明之电灯泡泡内有一一字形线圈灯丝,其所发之光穿过2公尺之105°—110℃水汽而交聚在分光仪之缝上。红外照相片经氨溶液之超度敏化后,即安置於已经配准之相片匣内,而使之感光。光之可见部分系用深红滤片割除。照光时间约 费四五十小时,然后除去滤片,照以水银光谱凡数秒,作为决定波长之标准。 用前法所摄得之光谱大都不十分清晰,其主要原因系由水汽管之太短。但用显微光度计量之,各成分线之波长不难准至1(?)范围以内。本实验所得各线若与五十年前Abney所测定太阳光谱中0.94μ附近之吸收线相比较,可见太阳红外光谱中许多吸收线系由大气中水汽所产生,而证实Abney最初之推想。惟本实验所测定之吸收线与Abney所测定太阳光谱中之对应黑线具有一等差数约合1.5(?)_0此等差数之产生想系由於波长单位之不同以及个别仪器误差所

A new method for the biological assay of vegetable purgatives based on the numbers of wet faeces excreted by groups of mice after dosing is described. The relation of the number of wet faeces per group of mice to the logarithm of the dose was found to be linear. A cage has been specially designed for this assay and it has been found advantageous to incorporate a definite proportion of water in the diet during test. 40 mice divided equally into 4 groups were used in each assay. 2 groups received the standard...

A new method for the biological assay of vegetable purgatives based on the numbers of wet faeces excreted by groups of mice after dosing is described. The relation of the number of wet faeces per group of mice to the logarithm of the dose was found to be linear. A cage has been specially designed for this assay and it has been found advantageous to incorporate a definite proportion of water in the diet during test. 40 mice divided equally into 4 groups were used in each assay. 2 groups received the standard preparation and the other 2 groups received the test preparation. The standard deviation of a single determination based on 9 such assays was estimated to be 15.7 per cent. For rhubarb and its preparations, a“6-point”assay is advocated. With suitable restric-tion in the design of the assay, it is possible to calculate the potency by simple methods. Powdered crude drugs are used as laboratory standards in the assay of senna and rhubarb. The doses of cascara bark required to produce distinctive responses are too inconveniently large to be administered in suspension. It was found possible to use a potent extract of cascara in place of the powdered bark as a laboratory standard. Examples of the assay and the subsequent calculations are given. The method described is not only convenient in use but also gives a comparatively high degree of accuracy. The method has been successfully applied to senna leaf, senna fruit, rhubarb, cascara sagrada and extracts and commercial preparations made from these drugs, pure glycosides(sennosides A and B) and pure anthracene compounds(aloe emodin and aloe-emodine anthranol).

(1)本文详述植物性泻药的一种新的生物测定法,此法係用小白鼠在服药后所排出的濕粪数为基础,以定泻药的效价。(2)小白鼠服药後所排出的湿粪数与剂量指数的关係经证明为一直线。(3)本法所用鼠笼係特别设计,并证明在饲料内加入一定量的饮水,具有多种优点。(4)番泻效价的测定,每次用小白鼠4组,每组10只。2组给与标准品,另外2组给与试验品。根据9次试验的结果,试验的标准差是15.7%.(5)大黄效价的测定,以采用“6点”法为宜,即每次试验用小白鼠6组,3组给与标准品,另外3组给与试验品,所得的准确度与上述相仿。波希鼠李皮浸膏的效价测定,则用“4点”法或“6点”法均可。(6)所有试验一律采用粉状生药为实验室的比较标准,但是波希鼠李皮的效价太低,它的粉末不适於作为标准之用,可用波希鼠李皮乾浸膏来代替,作为比较标准。(7)本文对於效价测定及其计算方法都举例说明,并介绍了比较常法为简捷的相关效价计算法。(8)本法不但方便易行,而且有相当高的准确度;曾用在番泻、大黄、波希鼠李皮及其制剂,以及一些纯粹的蒽醌衍生物的效价测定,都获得了满意的结果。

In view of the necessity of a rapid and accurate process for the deter-mination of fluorine applicable in the analysis of sodium fluoride and otherfluorine compounds,the author has established a new volumetric processconsisting in the titration in aqueous-alcoholic medium with ferric nitrate asstandard solution and sodium salicylate as indicator.All of the methods,published by Guyot,Greeff,Fairchild andVisintin proposed for the determination of fluorine using ferric solutionas standard,are based on the reaction:6NaF+FeCl_3→Na_3FeF_6+3NaCl....

In view of the necessity of a rapid and accurate process for the deter-mination of fluorine applicable in the analysis of sodium fluoride and otherfluorine compounds,the author has established a new volumetric processconsisting in the titration in aqueous-alcoholic medium with ferric nitrate asstandard solution and sodium salicylate as indicator.All of the methods,published by Guyot,Greeff,Fairchild andVisintin proposed for the determination of fluorine using ferric solutionas standard,are based on the reaction:6NaF+FeCl_3→Na_3FeF_6+3NaCl. But the sodium ferric fluoride thus formed is fairly soluble in water and makesthe end-point unclear,therefore the titration can not be performed accurately.This seems to be due to the fact that the following two reactions advancesimultaneously,and accordingly the formation of sodium ferric fluoride is in-complete in aque(?)us medium:3NaF+Fe(NO_3)_3→FeF_3+3N_aNO_33NaF+FeF_3→Na_3FeF_6Nevertheless,these reactions,according to the author's experiments;proceedalmost quantitatively in meda.containing at least 50% by volume of alcohol.This paper reports the xperimental results obtained in the fundamentalstudies on the various factors influencing the accuracy of the volumetry,namely,the sensitivity and the necessary amount of sodium salicylate used asindicator,the pH value,the alcoholic concentration of the titration medium,the concentration of the fluoride taken for the determination and the timewhen alcohol should be added in the course of titration.Furthermore,a rapidvolumetric process with high accuracy is proposed together with its applicationsin ordinary analyses of sodium fluoride and other fluorine compounds.The proposed method is characteristic in using sodium salicylate asindicator,which shows sharp violet color with minute amount of ferric ion inmedium of pH 3 controlled with buffer solution,then titrating with standardferric nitrate,and adding proper amount of alcohol(the alcoholic concentra-tion at the end-point should be above 50%)during the titration,when themedium becomes orange yellow in color.The method may be summarized as follows:Take 5 ml of neutral sodiumfluoride solution of about 0.3 N in a small Erlenmeyer flask,add 2.5 mlof Walpole's buffer solution of pH 3(formed by dissolving 34.0 g ofcrystalline sodium acetate and 20 ml of 38% HCl in water,and making upto 250 ml)and 1 ml of 0.1 M sodium salicylate dissolved in 50% alcohol.After sufficient stirring,titrate with standard 0.3 N(0.05 M)ferric nitratesolution,using micro-burette until the medium becomes orange yellow,thisstep being reached after addition of about 4 ml of titrant.Then decolorizethe solution by adding 12.5 ml of absolute alcohol(or 13 ml of 95% alcohol),previously purified by redistillation with lime;stirring is necessary during theaddition.Further continue the titration until the light pink color formeddoes not fade after stirring for 30 seconds when observed over a white surface. In the analyses of sodium fluoride and other fluorine compounds con-taining interfering substances,such as divalent and polyvalent metallic ions,phosphate,silicate,borate,carbonate,sulfide ions and reductants acting on ferricion,it is necessary to separate fluorine from these interfering substances bythe distillation with sulfuric acid according to the method of Willard andWinter(20).Then the distillate is neutralized with dilute sodium hydroxideand adjusted to the proper pH with hydrochloric acid using p-nitrophenol asindicator.The solution is ready for titration as described.But in the caseof absence of these interfering substances except carbonate,for example,inthe determination of the concentration of sodium fluorde solution obtained bythe extraction of the crude product,produced industrially by fusing fluorsparwith sodium carbonate and silica,the above separation of fluorine by dis-tillation is dispensable.The anaIytical results obtained by the proposed method are in goodagreement with those obtained by the lead chlorofluoride process(8),whichis recognized as official method for the determination of fluorine in agriculturalproducts.

本文介绍一容量分析氟的新方法和在工业制品上的应用,并分析了一种工业制备的氟化钠液,所得的结果和氟氯化铅法所得的极为一致。对于影响该分析法准确度的各种因素:指示剂的灵敏度和滴定时适宜的用量、溶液的 pH 值、应加的乙醇量、操作中加乙醇的次序、以及氟离子的适宜浓度,均加以研究并找出适宜的情况。本法用硝酸铁为标准液,水杨酸钠作指示剂,在 pH=3左右作滴定;当溶液呈橙黄色时,加入适量的乙醇,使其浓度在终点时仍不低于50%。如有干扰物质如二价及多价金属离子、磷酸根、矽酸根、硼酸根、碳酸根、硫化物和还原物质可能与三价铁起作用者,均应分离之。

 
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