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钒-硅酸锆蓝色颜料
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    Effects of some technology factors were roughly investigated by solid state reaction method. XRD and UV-V spectra analysis were applied to identify the samples and understand the results.
    探讨了工艺因素对钒 -硅酸锆蓝色颜料合成的影响 ,用XRD和UV -V光谱对样品进行了表征 ,得到一些有益的结论
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Effects of some technology factors were roughly investigated by solid state reaction method.XRD and UV-V spectra analysis were applied to identify the samples and understand the results.

探讨了工艺因素对 -硅酸锆蓝色颜料合成的影响 ,用XRD和UV -V光谱对样品进行了表征 ,得到一些有益的结论

Marker Technique was introduced to investigate ionic diffusion as well as formation mechanism of vanadium-zircon blue pigments.The result shows only Si\+\{4+\} is a motivable ion,which must be transported to zirconia site first and then,react with it to give zircon.And its transportation mainly depended on a melt formed from heating a mixture of NH\-4VO\-3 and NaF,although NaF also has effect on formation of glassy SiO\-2 which make it possible to transport Si\+\{4+\} throgugh liquid phase.Dissolution of zirconia...

Marker Technique was introduced to investigate ionic diffusion as well as formation mechanism of vanadium-zircon blue pigments.The result shows only Si\+\{4+\} is a motivable ion,which must be transported to zirconia site first and then,react with it to give zircon.And its transportation mainly depended on a melt formed from heating a mixture of NH\-4VO\-3 and NaF,although NaF also has effect on formation of glassy SiO\-2 which make it possible to transport Si\+\{4+\} throgugh liquid phase.Dissolution of zirconia is another important factor on producing of zircon,which rely on the decomposition of an unstable compound named ZrV\-2O\-7 formed from a reaction between ZrO\-2 and V\-2O\-5.

标志法用来研究 -硅酸锆蓝色颜料形成过程中的离子移动问题 ,借此了解该颜料的生成机理。结果表明Si4 + 和Zr4 + 中Si4 + 是唯一可以移动的离子 ;NaF的加入有利于SiO2 的玻璃化 ,因而对硅离子的迁移有一定贡献 ,但其移动更依赖于NaF和NH4 VO3反应所形成的液相。此外 ,ZrO2 的溶解也是硅酸锆生成的一个限制因素

 
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