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溶媒转换
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  change solvent
     The six factors that may affect micronization of Synthetic Broneol were experimentally observed in three levelsby L18(3 7), design of orthogonal test and change solvent.
     采用正交试验法与溶媒转换法,对可能影响冰片微粉化的6个因素,在3个水平上进行试验考察,并对试验结果进行方差分析。
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     转换
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     On the Converting Scales
     浅析进制的转换
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     Study on the solubility of griseofulvin in solvents
     灰黄霉素提取溶媒的研究
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  change solvent
The use of temperature as a variable in liquid chromatography enables the facile alteration of eluotropic strength without the need to change solvent composition.
      


The six factors that may affect micronization of Synthetic Broneol were experimentally observed in three levelsby L18(3 7), design of orthogonal test and change solvent. The result of variance analysis shows that , the best conditions of technology are: the stir speed is 400 r/min; the volume of added water is 80 ml; the speed of dropping water is 7 ml/min; the temperature of vacuum dryness is 30℃ ; 1 % magnesium stearate was added befor dropping waterl the used volume of alcohol is 15 ml(volume of dissolving...

The six factors that may affect micronization of Synthetic Broneol were experimentally observed in three levelsby L18(3 7), design of orthogonal test and change solvent. The result of variance analysis shows that , the best conditions of technology are: the stir speed is 400 r/min; the volume of added water is 80 ml; the speed of dropping water is 7 ml/min; the temperature of vacuum dryness is 30℃ ; 1 % magnesium stearate was added befor dropping waterl the used volume of alcohol is 15 ml(volume of dissolving 10. 0 g synthetic Broneol). The verfiable experiment of the optimum seeking technoloy shows the optimumseeking technology is believable.

采用正交试验法与溶媒转换法,对可能影响冰片微粉化的6个因素,在3个水平上进行试验考察,并对试验结果进行方差分析。方差分析结果表明,冰片微粉化的最佳工艺条件是:搅拌速度为400r/min;加水量为80ml;滴水速度为7ml/min;真空干燥温度为30℃;滴水前加入1%硬脂酸镁;乙醇用量为15ml(溶解10.0g冰片的量)。采用优化工艺的验证试验表明,优选工艺是可信的。

The optimum synthetic condition for (9-Fluorenly)methanol is discussed in this article.The methor of solvent comversion is also discussed at the same time.

本文讨论了芴甲醇合成条件的优化设计,利用溶媒转换法从母液中分离出产品的方法。

 
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