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   solid phase extraction 在 药学 分类中 的翻译结果: 查询用时:0.187秒
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solid phase extraction
相关语句
  固相萃取
    FLURESCENCE DETERMINATION OF PROPANOLOL IN THE SERUM WITH SOLID PHASE EXTRACTION
    血清中普萘洛尔的固相萃取及荧光法测定
短句来源
    Quantitative analysis of pramocaine and butacaine in blood by capillary gas chromatography with solid phase extraction
    固相萃取和毛细管气相色谱法定量测定血中普莫卡因和布他卡因
短句来源
    Determination of mycophenolic acid in plasma by reversed phase high performance liquid chromatography with solid phase extraction
    固相萃取反相高效液相色谱法测定人血浆麦考酚酸浓度
短句来源
    HPLC Determination of Salbutamol in Human Plasma by Solid Phase Extraction
    固相萃取高效液相色谱法测定人血浆中的沙丁胺醇
短句来源
    Simultaneous Determination of Acemetacin and Its Metabolite Indomethacin in Human Plasma by Solid Phase Extraction HPLC with UV Detection
    人血浆中阿西美辛及其代谢物吲哚美辛的固相萃取-HPLC-UV法测定
短句来源
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  固相萃取法
    METHODS Plasma samples were pretreated by solid phase extraction. Cefpodoxime and cefuroxime (internal standard) were separated on M N Necleosil 100 5 C 18 column( 150 mm × 4.6 mm , 5 μm )at 39 ℃ with 0.05 mol ·L -1 acetate buffer of pH 3.8 methanol(82∶18)as mobile phase at a flow rate of 1 mL ·min -1 , and monitored at 234 nm .
    方法 :采用固相萃取法预处理血浆样品 ,分析柱为M N Necleosil 10 0 5C18柱 (15 0mm× 4 .6mm ,5 μm) ,流动相为pH 3.8的 0 .0 5mol·L-1醋酸缓冲液 甲醇 (82∶18) ,流速为 1mL·min-1,检测波长为 2 34nm ,柱温为 39℃ ,按内标法定量。
短句来源
    A C18column was usesd with the mobile phase of methanol-water-triethylamine- acetic acid (600∶400∶ 4∶2) at the detectionwavelength of 254nm. The blood was extracted with solid phase extraction, using diazepam as internal standard.
    采用C18柱,流动相为甲醇-水-三乙胺-乙酸(600∶400∶4∶2),检测波长254nm,固相萃取法处理血样,地西泮为内标。
短句来源
    OBJECTIVE:To extract the antiepilepsy drugs in plasma by solid phase extraction(SPE).
    目的:探讨固相萃取法用于血浆中抗癫痫药物的提取。
短句来源
    Objective To establish solid phase extraction method for plasma and bronchoalveolar lavage fluid (BAL) sample preparation and determination of cefixime with RP HPLC.
    目的 建立反相固相萃取法 ,用于血浆和支气管肺胞灌流液 (BAL)中头孢克肟 (CFX)浓度测定的准备 ,并以HPLC法测定CFX含量。
短句来源
    METHODS A solution of prednisone as the internal standard was added to a 0.2 mL plasma aliquot. The resulting sample was treated with water and dilute HCl and applied to a C 18 solid phase extraction column,a C 18 column (7 μm particle size,250 mm×4.6 mm ID) was used with the temperature at 40℃.
    方法 用固相萃取法处理样品 ,以泼尼松为内标物 ,C18硅胶键合相为固定相 ,甲醇 四氢呋喃 水 (6 0∶2∶5 0 )作流动相 ,在波长 2 5 4nm处紫外定量检测。
短句来源
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  “solid phase extraction”译为未确定词的双语例句
    The application of solid phase extraction for systematic toxicological analysis of abuse drugs
    固根萃取技术在系统药、毒物分析中的应用
短句来源
    Method:To extract the ofloxacin in serum by solid phase extraction with C18 SPE column , then to separate and determine the enantiomers of ofloxacin in serum by high performance liquid chromatography with chiral mobile phase additive, using L–isoleucine as the chiral additive,Cu2+ as the ligand ion.
    方法:以L-异亮氨酸为配合剂,Cu2+为配合离子,采用高效液相色谱手性流动相添加剂法测定血中氧氟沙星对映体的含量。
短句来源
    RESULTS:The average recovery was 96.95%±s 7.59 % for SPE(solid phase extraction) procedure in serum. The drug time curve of sinomenine in rabbits was determined.
    结果:血清中青藤碱的固相提取回收率为96.95%±s7.59%,用薄层扫描法测绘了2只家兔静注青藤碱后的药物浓度时间曲线。
短句来源
    The metabolites of salmeterol(M1-M4) were identified by LC/MS/MS after solid phase extraction followed by enzyme hydrolysis and GC/MS after derivatization. Mass spectrometry was operated in the positive mode for the method of LC/MS/MS.
    方法:ig给药后,收集小鼠尿液,经固相提取,葡萄糖醛酸酶水解,进行LC/MS/MS分析和硅烷化后进行GC/MS分析同时分离鉴定沙美特罗代谢产物。
短句来源
    Objective:To develop a sensitive and specific solid phase extraction (SPE)-HPLC method for detec- ting geldanamycin in Beagle dog plasma and to study its pharmacokinetics in Beagle dogs by iv injection.
    目的:建立格尔德霉素在 Beagle 犬血浆中的同相萃取(SPE)-HPLC 测定方法,并研究其在犬体内的药代动力学。
短句来源
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  solid phase extraction
A sample pretreatment microfluidic chip was described based on the principle of solid phase extraction and micro electro mechanical system technology.
      
LC-18 column was employed in solid phase extraction (SPE), 1.0 mL of hexane was adopted in liquid-liquid extraction (LLE), and the extracts were analyzed by gas chromatograph mass spectrum (GCMS) in selected ion mode.
      
Solid Phase Extraction and Spectrophotometric Determination of Silver with 2-(2-Quinolylazo)-5-Dimethylaminophenol
      
The method is based on the rapid reaction of silver(I) with QADMAP and the solid phase extraction of the colored chelate using a C18 cartridge.
      
This chelate was enriched by solid phase extraction with C18 cartridge, and the retained chelate was eluted from the cartridge using ethanol (with 1% acetic acid).
      
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Leukotriene B^, a metabolite of arachidonic acid via 5-lipoxygenase, is a potent mediator in inflammatory reactions. The RP-HPLC was ernptoyed for measuring L-TB4 generated from rabbit whole blood and polymorphoneuclear leukocytes. We evaluated ,the effects of inethanol concentration, PH and plasma protein on the solid-phase extraction of LTB4 ia biological samples. Simple and practical techniques were developed.

白三烯B_4(LTB_4)系花生四烯酸的5-脂氧酶代谢产物,是炎症反应中的重要介质。本文建立了测定白细胞及兔全血来源白三烯B_4的反相高效液相色谱法, 研究了样品介质的pH、甲醇浓度及血浆蛋白等对生物样品中LTB_4固相萃取的影响,建立了简便实用的萃取和测定方法

A simple and sensitive method for the determination of methandienone and its metabolite in human urine by HPLC, using methyotestosterone as internal standard, was developed. The urine sample was first purified by solid phase extraction method, and then determined by HPLC with detective wavelength at 254 nm. The mobile phase was methanol-water (100: 40 V/V). It showed a good linearity between the range of 0.05~1.0 μg/ml with the correlation coefficient of 0.9993. The detective limit was 5 ng, and...

A simple and sensitive method for the determination of methandienone and its metabolite in human urine by HPLC, using methyotestosterone as internal standard, was developed. The urine sample was first purified by solid phase extraction method, and then determined by HPLC with detective wavelength at 254 nm. The mobile phase was methanol-water (100: 40 V/V). It showed a good linearity between the range of 0.05~1.0 μg/ml with the correlation coefficient of 0.9993. The detective limit was 5 ng, and the sensitivity was 25 ng/ml. The precisions of both within-day and day-to-day were less than 5%. This method was found to be much simpler and more inexpensive than that of GC-MS, and it could serve as an alternative method for the doping control in athletes training.

本文建立了尿中去氢甲基睾丸素及其代谢物的HPLC分析方法。尿样以固相法在XAD-2树脂柱上提取纯化后再经HPLC分析。检测波长为254 nm,流动相为甲醇-水(100:40V/V)。当尿中药物浓度在0.05~1.0μg/ml时,方法线性关系良好,相关系数为0.9993。本法检测限为5 ng,灵敏度为25ng/ml,日内、日间误差均小于5%。

A simultaneous analysis of nitrazepam, clonazepam, and flunitrazepam in human urine by SepPak solid-phase extraction and RP-HPLC is presented.Within-day and day-day precision are about.1-5%.It is sensitive and can be used in clinical and toxic kinetic studies.

本文介绍了一种用SepPak固相萃取技术和HPLC同时检验尿液中的苯并二氮草类药物硝基安定、氯硝基安定和氟硝基安定的方法。使用的反相色谱柱为YMC A—303C_(18)柱,以乙腈—0.01M醋酸铵(45:55,V/V)为流动相,紫外检测波长为254nm。各药物的回收率均大于80%;日内和日间测定的变异系数为1—5%。

 
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