In view of these facts, this product may be used as a medical preparation. The product with mp 143~145℃, reported in literature showed a loss on drying of more than 2%. It contains approximately 93% C_(16)H_(24)O_4NGl.
The moisture content of sample was quantified by a partial least square (PLS) calibration model, correlative spectrum calculation was used for wavelength selection and multiplicative signal correction (MSC) was applied for pretreatment in the calibration model. Primary reference data were obtained using the traditional loss on drying (LOD) method.
METHODS In order to establish a method for water content determination in tazobctam, many methods including Karl Fischer titration, weight loss on drying, TGA, DSC and X ray diffraction experiment of an orthorhombic form were studied.
In this paper, a new high-speed moisture determination balance based on the loss on drying method and the adaptive data fusion theory with shift sampling method is proposed. Consisted of the infrared oven and the electronic balance, the new moisture balance can precdict the sample's moisture content with high accuracy while the sample is still under drying.
This paper starts with two aspects which are to improve drying efficiency, quicken moisture escaping and information fusion prediction and explores a feasible and effective way to implement fast measurement of traditional loss on drying.
The simulation result is shown that it is expected to solve the problems such as a long time drying and the fussy operation during the traditional loss on drying.
In view of these facts, this product may be used as a medical preparation. The product with mp 143~145℃, reported in literature showed a loss on drying of more than 2%. It contains approximately 93% C_(16)H_(24)O_4NGl.
In the new standard, loss on drying was ≤30%, salt content was ≤8%, nitrite was ≤30 mg/kg, the inedxes of acid value and nitrate amount was discarded, the index of peroxide was used instead of acid value, whether malondialdehyde was used to be the index was not determined.
IR, 1H NMR, and UV spectra were obtained for cardiocyclide; its solubility was studied; its melting temperature, weight loss on drying and the transparency, color, and pH of its solutions were determined.
Flowability, true and tap density, loss on drying, particle size, specific surface area and scanning electron micrographs were used to characterize these powders with low compaction pressures (lower than 10 MPa).
Determination of loss on drying or consistency of opium samples using microwave ovens.
例句来源
There is a difference in melting point between the product Kěbiding (4-morpholino-ethyl ester of 2-methyl-2-phenoxypropanoic acid hydrochloride) with mp 154~155℃ synthesized in this laboratory and the product morphethylbutyne with mp 143~145℃ reported in the Iiterature(1). Therefore, the quality of the drug was studied.Kěbiding was synthesized by esterification of 4-morpholinoethanol with 2-methyl-2-phenoxypropanoyl chloride or 2-methyl-2-phenoxypropanoic acid by the authors. It possesses mp 154~155℃. This ...
A RP-HPLC was used to determination the content of Paeenifl orin (Ⅰ) and glycyrrhizin (Ⅱ)in Baiheguj intang Granule. Using this method, Ⅰ and Ⅱ were isoluted well and other composi tions in Baihegujintang Granule didn't interfere the assay, the variations in the day were 1.27% (Ⅰ) and 0.92% (Ⅱ) , day to day were 1.91% (Ⅰ) and 2.35%(Ⅱ), the average recovery were 102.3% (Ⅰ) and 99.85% (Ⅱ) respectively. The contents ofthree batches were 1.13‰-1.21‰ (Ⅰ)and 3.33‰-7.02‰ (Ⅱ) respectively.Fxception the contents of ...
Objective: To apply microwave technique to determin the loss on drying of chemicals. Methods: The effects of microwave power, drying time and the number of the samples on the rate of drying have been investigated. In addition, the loss on drying of organic chemicals including sodium benzoate and quinine sulfate and inorganic chemicals including sodium carbonate and calcium sulfate consisting of free water or combined water has been determined by the micr...