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xiancaihuangliansu
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  苋菜黄连素
     Determination of Berberine in xiancaihuangliansu Capsule by HPLC
     高效液相色谱法测定苋菜黄连素胶囊中盐酸小檗碱的含量
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     OBJECTIVE To establish a rapid and accurate method for detemining berberine in xiancaihuangliansu capsule by HPLC.
     目的建立了一种快速、准确的高效液相色谱法测定苋菜黄连素胶囊中盐酸小檗碱的含量的方法。
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     CONCLUSION The method is simple and rapid,the results is accurate and good reproducible. It can be used control the qulity of berberine in xiancaihuangliansu capsule.
     结论试验结果表明本法简便快速,重现性好,结果准确可靠,可以作为苋菜黄连素胶囊中盐酸小檗碱含量测定的方法。
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  相似匹配句对
     Determination of Berberine in xiancaihuangliansu Capsule by HPLC
     高效液相色谱法测定苋菜黄连素胶囊中盐酸小檗碱的含量
短句来源
     OBJECTIVE To establish a rapid and accurate method for detemining berberine in xiancaihuangliansu capsule by HPLC.
     目的建立了一种快速、准确的高效液相色谱法测定苋菜黄连素胶囊中盐酸小檗碱的含量的方法。
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OBJECTIVE To establish a rapid and accurate method for detemining berberine in xiancaihuangliansu capsule by HPLC.METHODS The Chromatographic conditions included Hypersil ODS_2(5μm,250mm×4.6mm);the mobile phase was acetontrile and 0.033% potassium phossphate monobasic(45∶55);the flow rate was 1mL·min~(-1);the detection wavelength was 350nm;column temperature at room temperature.RESULTS There were good linear relationship for berberine with the range of 0.05μg~0.30μg,r=0.9999,the average recoveries were...

OBJECTIVE To establish a rapid and accurate method for detemining berberine in xiancaihuangliansu capsule by HPLC.METHODS The Chromatographic conditions included Hypersil ODS_2(5μm,250mm×4.6mm);the mobile phase was acetontrile and 0.033% potassium phossphate monobasic(45∶55);the flow rate was 1mL·min~(-1);the detection wavelength was 350nm;column temperature at room temperature.RESULTS There were good linear relationship for berberine with the range of 0.05μg~0.30μg,r=0.9999,the average recoveries were 99.86%,RSD= 1.07%(n=9).CONCLUSION The method is simple and rapid,the results is accurate and good reproducible.It can be used control the qulity of berberine in xiancaihuangliansu capsule.

目的建立了一种快速、准确的高效液相色谱法测定苋菜黄连素胶囊中盐酸小檗碱的含量的方法。方法色谱柱HypersiL ODS2(5μm,250mm×4.6mm)流动相:乙腈-0.033%磷酸二氢钾(45∶55);流速:1mL.m i-n 1;检测波长:350nm;柱温:室温;进样量:20μL。结果盐酸小檗碱进样量在0.05μg~0.30μg范围内线性良好,r=0.9999。平均回收率为99.86%,RSD=1.07%(n=9)。结论试验结果表明本法简便快速,重现性好,结果准确可靠,可以作为苋菜黄连素胶囊中盐酸小檗碱含量测定的方法。

 
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