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参比极
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     Taken Fe/FeO as reference electrode, the oxygen partial pressure was measured, and standard free enthalpy of formation of non-stoichiometric FeO (w/istite) was obtained as ΔG_(FeO)~0=-259030+60.25T (J·mol~(-1)).
     选用Fe/FeO为参比极,测得其氧分压,并求出非化学计量FeO的标准自由焓ΔG°FeO=-259030+60.25T(J·mol~(-1))。
短句来源
     Needle concentration cells for oxygen measurement of liquid steel, were made by Plasma torch spray coating technique, in which Mo/MoO_2 was used as reference and ZrO_2 (4%CaO) as electrolyte. It could be expressed as following:Mo ? Mo/MoO_2||ZrO_2(4%CaO)||[O]-Fe ?
     用等离子火焰喷制的,以Mo/MoO_2为参比极,ZrO_2(4%CaO)为电解质的针式定氧电池,其电池结构为Mo·Mo/MoO_2‖ZrO_2(4CaO)‖[O]-Fe·Mo,电解质厚度为0.3mm。
短句来源
     A sulphur sensor of high melting point was developed taking MgS + ZrS2 as solid electrolyte and Mo+MoS2 as reference electrode, i.e.Mo|Mo+MoS2||MgS+ZrS2||[S]Fe|MoThe determination of sulphur content in liquid iron was carried out at 1 638 K (1365℃) in atmosphere.
     应用特殊方法自行合成了MgS,ZrS_2,MOS_2,WS_2和TiS_2等高熔点硫化物。 以MgS+ZrS_2作为固体电解质,以Mo+MoS_2作为参比极,组成定硫探头:Mo|Mo+MOS_2‖MgS+ZrS_2[S]_(Fe)|Mo,在大气气氛下,于1638K,测定了铁水[S]含量。
短句来源
     The tubular-type oxygen sensors fabricated by thermal-press technique can continuously measure in steel melts at 1600℃ for 3.5 hours(Mo/ MoO_2 used as reference electrode)and 5 hours (Cr/Cr_2O_3 used as reference electrode).
     用热压铸成型方法制成的单向增厚管状长寿命定氧测头,在1600℃的钢液中,用Mo/MoO_2为参比极可连续稳定测量3.5h,而用Cr/Cr_2O_3为参比极,则可连续稳定测量5h。
短句来源
     The oxygen probe made speclally,sealed by refractory cement and adopting ZrO_2 base solid electrolyte tube, reference electrode with Cr. Cr_2O_3 powders,Mo electrode lead wire,has a good measuring stability. By experiments,the oxygen potential for high TiO_2 containing blast fur-nace slag is determined,uccesxfully.
     采用ZrO_2基的固体电解质管,参比极选用Cr,Cr_2O_3粉,电极引线用Mo丝,用高温水泥封装特制的定氧探头具有良好的稳定住,实验测定含钛高炉渣的氧势是成功的。
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An electrochemical cell based on ZrO2 and HfO2 and intended for investigation of glass-forming melts with the use of a platinum electrode and a reference electrode with oxygen-ion conductivity was designed and fabricated.
      
A procedure was proposed for the determination of selenium(IV) by stripping voltammetry on a mercury-film electrode at an electrolysis potential of +0.4 V versus the saturated silver-silver chloride reference electrode in a 1 M H2SO4 solution.
      
On the Location of a Reference Electrode for Electrochemical Measurements on an Underground Pipeline
      
The method of direct potentiometry was applied to measure redox potentials of Sm3+/Sm2+ and Eu3+/Eu2+ in molten cesium chloride relative to chlorine reference electrode in the temperature range 973-1173 K.
      
The general principle of operation of electrochemical sensor Me, Pb/PbCl2-CaCl2/Pb1 ± δS, is based on measuring EMF of an electrochemical circuit with a lead-conducting electrolyte at a specified sulfur vapor pressure above the reference electrode.
      
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The oxygen partial pressure and activity of FeTiO_3-MgTiO_3 solid-solution system were studied by means of oxygen concentration cell with the solid electrolyte. Taken Fe/FeO as reference electrode, the oxygen partial pressure was measured, and standard free enthalpy of formation of non-stoichiometric FeO (w/istite) was obtained as ΔG_(FeO)~0=-259030+60.25T (J·mol~(-1)). Furthermore, the oxygen partial pressure and wustite activity of the various compositions of the solid-solution system were measured at the...

The oxygen partial pressure and activity of FeTiO_3-MgTiO_3 solid-solution system were studied by means of oxygen concentration cell with the solid electrolyte. Taken Fe/FeO as reference electrode, the oxygen partial pressure was measured, and standard free enthalpy of formation of non-stoichiometric FeO (w/istite) was obtained as ΔG_(FeO)~0=-259030+60.25T (J·mol~(-1)). Furthermore, the oxygen partial pressure and wustite activity of the various compositions of the solid-solution system were measured at the temperature range of 900—1200℃. The results show that both values increase with the increase of temperature. The standard free enthalpy of formation of complex oxide FeTiO_3, ΔG_(FeTiO_3)~0=-40470+19.75T (J·mol~(-1)) and the activity-composition relation of this solid-solution series were obtained.

采用固体电解质氧浓差电池研究了FeTiO_3-MgTiO_3固溶体系的氧分压和活度。选用Fe/FeO为参比极,测得其氧分压,并求出非化学计量FeO的标准自由焓ΔG°FeO=-259030+60.25T(J·mol~(-1))。测定了固溶体系不同组成,在900—1200℃区间的氧分压和FeO的活度。其结果表明,二者均随温度的升高而增加。将数据处理后,得到生成复合氧化物FeTiO_3的标准生成自由焓,ΔG°FeTio_3=-40470+19.75T(J·mol~(-1))以及固溶体的组元活度与组成的关系图。

Needle concentration cells for oxygen measurement of liquid steel, were made by Plasma torch spray coating technique, in which Mo/MoO_2 was used as reference and ZrO_2 (4%CaO) as electrolyte. It could be expressed as following:Mo ? Mo/MoO_2||ZrO_2(4%CaO)||[O]-Fe ? Mo The thickness of electrolyte was 0.3mm. The reliability, reproducibility and accuracy were investigated in laboratory scale. 34 cells made at different time were used for measuring one by one. 27 cells divided into three groups (9 Cells in each)...

Needle concentration cells for oxygen measurement of liquid steel, were made by Plasma torch spray coating technique, in which Mo/MoO_2 was used as reference and ZrO_2 (4%CaO) as electrolyte. It could be expressed as following:Mo ? Mo/MoO_2||ZrO_2(4%CaO)||[O]-Fe ? Mo The thickness of electrolyte was 0.3mm. The reliability, reproducibility and accuracy were investigated in laboratory scale. 34 cells made at different time were used for measuring one by one. 27 cells divided into three groups (9 Cells in each) which were taken for measuring three different oxygen levels. The mean coefficient of variation is 3.54%; the oxygen activity with different carbon content in the bath of pure liquid Fe was measured. It shows that the result is in better agreement with C-O eqeilibrium curve than chemical analysis. In addition, the partial electron conductivity parameter Pe'was determined. At 1600℃, lg Pe'=-14.5.

用等离子火焰喷制的,以Mo/MoO_2为参比极,ZrO_2(4%CaO)为电解质的针式定氧电池,其电池结构为Mo·Mo/MoO_2‖ZrO_2(4CaO)‖[O]-Fe·Mo,电解质厚度为0.3mm。在实验室于钼丝炉内,用氩气保护下氧化铝坩埚中的500g钢液,对电池的测成率、再现性和准确性进行了考察。对不同时间喷制的34支电池进行了连续测量。选取三组各9支电池对三种氧水平进行测定,平均波动系数σ=α_0测α_0/α_0=±3.54%;在纯铁液(Fe>99.8%)中,逐渐改变碳含量,测量其氧活度变化,与化学分析值相比,与理论曲线吻合得更好。此外,用抽氧法测量了P_e/o在1600℃时1gPe/o=-14.5。

A sulphur sensor of high melting point was developed taking MgS + ZrS2 as solid electrolyte and Mo+MoS2 as reference electrode, i.e.Mo|Mo+MoS2||MgS+ZrS2||[S]Fe|MoThe determination of sulphur content in liquid iron was carried out at 1 638 K (1365℃) in atmosphere. Furthermore, to determine the characteristic partial pressure of sulphur in MgS+ZrS2 solid electrolytes, another sulphur sensor was developed taking Mo + MoS2 as reference electrode and W+WS2 as the electrode to be measured with partial pressure of...

A sulphur sensor of high melting point was developed taking MgS + ZrS2 as solid electrolyte and Mo+MoS2 as reference electrode, i.e.Mo|Mo+MoS2||MgS+ZrS2||[S]Fe|MoThe determination of sulphur content in liquid iron was carried out at 1 638 K (1365℃) in atmosphere. Furthermore, to determine the characteristic partial pressure of sulphur in MgS+ZrS2 solid electrolytes, another sulphur sensor was developed taking Mo + MoS2 as reference electrode and W+WS2 as the electrode to be measured with partial pressure of sulphur given, i.e.Mo|Mo+MoS2||MgS + ZrS2||W+WS2|MoThe experimental results show that both the sensors developed are available to determine [S] content in liquid iron.

应用特殊方法自行合成了MgS,ZrS_2,MOS_2,WS_2和TiS_2等高熔点硫化物。以MgS+ZrS_2作为固体电解质,以Mo+MoS_2作为参比极,组成定硫探头:Mo|Mo+MOS_2‖MgS+ZrS_2[S]_(Fe)|Mo,在大气气氛下,于1638K,测定了铁水[S]含量。以Mo+MOS_2和W+WS_2作为已知硫分压的参比极和被测极组成定硫探头:Mo|Mo+MoS_2‖MgS+ZrS_2|W+WS_2|Mo,测定了MgS+ZrS_2固体电解质的特征硫分压P_e~'(s)。试验结果表明,新开发的定硫探头可用于测定铁水[S]含量。

 
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