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  tablets
Analytical results for two batches of compound ibuprofen tablets by the SEKI-based FI-CE approach were in good agreement with that obtained by a conventional high performance liquid chromatographic method.
      
Sulfanilamides were determined in Pharmaceuticals (tablets, ointments, and drops) and biological fluids (protein hydrolyzates, urine, blood serum, and whole blood).
      
The proposed method has been successfully applied for the determination of DPH, LD and MD in injections and tablets of pharmaceutical preparations.
      
Sulfanilamides were determined in medicinal forms (tablets, ointments, and drops) and biological fluids (protein hydrolyzate, blood plasma, and whole blood).
      
Finally, this method was used in the analysis of the vitamin C content of different pharmaceutical preparations, such as multivitamin tablets and syrups, vitamin-C tablets and powders, and effervescent tablets.
      
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Commonly used alkaloidal salts may be titrated accurately with acetous HClO_4 in non-aquous media in semi-micro scale using crystal violet as visual indi- cator.The method gave results compared favorably with those obtained by usual method in the respect of its simplicity,rapidity and reproducibility. A modified method was suggested to facilitate the extraction of alkaloidal salts as such from tablets by means of water,aqueous alcohol or other strong polar solvents.

1.作者对常用的生物碱类药物及其注射剂片剂,试用半微量非水溶液滴定法进行测定其含量.所得结果与药典方法测得者均能相近.2.非水溶液滴定法极简捷,结果准确.可能代替药典中若干药物的法定含量测定方法,但须注意杂质影响.3.用水或醇自片剂中半微量法滤出有效成分,直接滴定,方法简便,可得满意结果.

Solutions of potassium antimony tartrate and sodium antimony gluconate were given per os to infected rabbits.Although their oral dosages were,respectively,9 and 4 times as much as their intravenous ones,the therapeutic results of the oral groups were far inferior to those of intrave- nous groups,while the animal mortalities of the former decidely higher than those of the later. In similar doses,one preparation (kindly supplied to us by Hsing Hwa)of the enteric tablets of potas- sium antimony tartrate was...

Solutions of potassium antimony tartrate and sodium antimony gluconate were given per os to infected rabbits.Although their oral dosages were,respectively,9 and 4 times as much as their intravenous ones,the therapeutic results of the oral groups were far inferior to those of intrave- nous groups,while the animal mortalities of the former decidely higher than those of the later. In similar doses,one preparation (kindly supplied to us by Hsing Hwa)of the enteric tablets of potas- sium antimony tartrate was tried and found to be useless,in view of its great potentialities the oral route of administration for antimony com- pounds is worth further and more intensive inves- tigation.

应用酒石酸锑钾与葡萄精酸锑~(Ⅲ)钠溶液的经口给药法,试治家兎血吸虫病,确有相当疗效。口服剂量虽较注射剂量分别加至九倍与四倍,但其疗效仍远不如注射法给药各组,而动物死亡率反较高。延长治程而酌减每次口服剂量,经口给药与静脉给药适当结合,仍不能提高其安全性。所试的酒石酸锑钾肠溶片在相同剂量时完全无效。口服锑剂的进一步研究应在吸收控制与剂型改进两方面努力。

Since 1954 in authors' laboratory, various digitalis preparations, including digitalis leaves, tablets and tinctures and digitoxin and its injections, were assayed by both guineapig method and pigeon (lethal dose) method, using standardized digitalis powder as reference standard. It was found that results of digitalis leaf preparations obtained by guinea pig method and those by pigeon method were reasonably agreeable; while the results of digitoxin preparations obtained by guinea pig method were always...

Since 1954 in authors' laboratory, various digitalis preparations, including digitalis leaves, tablets and tinctures and digitoxin and its injections, were assayed by both guineapig method and pigeon (lethal dose) method, using standardized digitalis powder as reference standard. It was found that results of digitalis leaf preparations obtained by guinea pig method and those by pigeon method were reasonably agreeable; while the results of digitoxin preparations obtained by guinea pig method were always significantly lower than those obtained by pigeon method. In this paper, these facts were again shown, when 6 digitalis leaf preparations and 7 commercial digitoxin preparations were investigated. In digitoxin preparations, the potency estimated by pigeon method could be 2.36 times greater than that estimated by guinea pig method. The authors ascribed the difference to the inadequate standard preparation employed in the assay, as digitalis purpurea consisting of chiefly purpurea glycosides A and B being different in the mode of action to digitoxin (commercial) which was chiefly degraded product of purpurea glycoside A. They concluded that in bioassay of digitoxin against a digitalis standard, a suitable authorised method should be strictly followed; and the 4 methods employing different kinds of animals recommended by British Pharmacopeia 1953 and quoted by Bristish Pharmacopeia Codex 1954 for digitoxin would make confusions.

1、本文用豚鼠法和鸽法比較了6种国产洋地黄粉、2种国产洋地黄毒甙和5种进口洋地黄毒甙的生物效价,用洋地黄粉作标准品。 2、洋地黄粉用两种方法測定的結果比較接近。洋地黄毒甙相差达一倍,鸽法的結果较高,此种較大的差异,显然是与样品和标准品在成分上的不同有关。 3、本文指出英国副藥典(1954)对洋地黃毒甙的检驗,叫种方法并列,并以洋地黄叶粉为标准品是有問題的。作者考虑到如果用一定純度的洋地黄毒甙作为生物检定的标准品时,各法可以并用,否則应按一种規定的方法进行。本室張淑坤、赵秀文、周海鈞三位同志曾参与本文一部分实驗工作。

 
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