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diclofenac
相关语句
  双氯芬酸
    A STUDY OF DETERMINATION OF DICLOFENAC SODIUM IN SERUM BY RP-HPLC
    RP-HPLC测定血浆中双氯芬酸钠的研究
短句来源
    SYNTHESIS OF DICLOFENAC SODIUM
    双氯芬酸钠合成研究
短句来源
    SYNTHESIS OF DICLOFENAC SODIUM FROM CYCLOHEXANONE
    双氯芬酸钠合成工艺研究
短句来源
    Studies on the Preparation and Pharmacokinetics of Diclofenac Sodium Sustained Release Capsules
    双氯芬酸钠缓释胶囊的制备及药代动力学
短句来源
    Study on Dissolution Test Methods for Diclofenac Sodium Suppository
    双氯芬酸钠栓溶出度测定方法的研究
短句来源
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  “diclofenac”译为未确定词的双语例句
    Study on New Process of Diclofenac Sodium
    双氯灭痛合成新工艺的研究
短句来源
    N-phenly-2, 2, 6. 6-tetrachlorocyclohexaneimine is a intermediate of diclofenac sbdium. The synthetic processes of N-phenly-2, 2. 6. 6-tetrachlorocyclohexaneimine were studied in this paper.
    本文对医药邻─(2,6─二氯苯胺基)─苯乙酸钠的中间体N─苯基─2,2,6,6─四氯环己亚胺的合成工艺进行了系统研究,对该反应的催化剂种类、用量、原料配比、缩合温度等。
短句来源
    A HPLC method for determination of metformin hydrochloride and glibenclamide in compound metforminhydrochloride tablets was established. Diclofenac sodium was used as the internal standard.
    建立了HPLC法测定复方盐酸二甲双胍片中盐酸二甲双胍和格列本脲的含量。
短句来源
    Three batches of (Ⅰ) contained not less than 95.0% and not more than 105.0% of the labeled amount of diclofenac potassium. Thier release percentage at 0.25 h, 6 h and 10 h was 20%~40%, 60%~80%and more than 80% of the label amount respectively.
    三批双层片在0.2h、5h、6h和10h的释放量均控制在标示量的20%~40%、60%~80%和80%以上。
短句来源
    The linear range of Diclofenac was in the range of 10.00~60.00μg,r=0.9999,and its average recovery was 99.7%(RSD=0.4%,n=9).
    双氯灭痛在10.00~60.00μg范围内呈线性关系,r=0.9999; 平均回收率:镇痛新为99.6%,RSD=0.4%(n=9);
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  diclofenac
Diclofenac (25 mg kg-1) and meloxicam (7.5 mg kg-1) produced 9.3 and 19.6 mm2 ulcer areas in stomachs of rats, respectively, when used alone, but when combined with nimesulide diclofenac and meloxicam did not cause any injury in rat stomachs.
      
While ranitidine at 100 mg kg-1 dose prevented diclofenac-induced ulcer formation, it reduced meloxicam-induced ulcer formation significantly.
      
Determination of diclofenac in pharmaceuticals and urine samples using a membrane sensor based on the ion associate of diclofena
      
The potentiometric response characteristics of a diclofenac selective electrode, based on ion association in different plasticizers, were compared.
      
The potentiometric unit presented a linear response toward diclofenac concentrations between 1 × 10-5 - 5 × 10-2 mol L-1, with slopes of approximately 60 mV dec-1, and exhibited a response time of 3 s.
      
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A simple, sensitive and reproducible RP-HPLC method was developed for the determiantion of diclofenac sodium (DS) in plasma. The samples were extracted by ether-dichloromethane in a pH5.0 HWc-NaAc buffer solution. A Gilson HPLC instrument, fitted with a YWG C8H17 10μm column (150×4.6mm) and a variable wavelength UV detector adjusted to 280nm, was used. The mobile phase contained of a mixture of MeOH and 0.02mol/L HAc 65:35(F/F). The flow rate was 1.0ml/min. Carbamazipine (CZ) was used as an internal standard....

A simple, sensitive and reproducible RP-HPLC method was developed for the determiantion of diclofenac sodium (DS) in plasma. The samples were extracted by ether-dichloromethane in a pH5.0 HWc-NaAc buffer solution. A Gilson HPLC instrument, fitted with a YWG C8H17 10μm column (150×4.6mm) and a variable wavelength UV detector adjusted to 280nm, was used. The mobile phase contained of a mixture of MeOH and 0.02mol/L HAc 65:35(F/F). The flow rate was 1.0ml/min. Carbamazipine (CZ) was used as an internal standard. A linear calibration curve for DS was measured within a range of 0.24μg 22.8μg/ml. The limit of detection was 3.6ng and the lower concentration for detection was 60ng/ ml. Good coefficient of correlation (Y=-33.75+792.24X, r =0.999 9) was obtained, and an the average CV% of within and betwean-days were 0.88% and 2.35% respectively (n= 5). The anti-inflammatory agents for the routine analysis of large numbers of plasma samples usually obtained in pharmacokinetic studies were suitable.

本文利用反相高效液相色谱法(RP-HPLC)对双氯芬酸钠(DS)血浓度的测定进行了研究,建立了灵敏、精确、简便、重现性好的分析方法。适用于药代动力学的研究。条件是在0.2mol/L NaAc-HAc缓冲溶液(pH5.0)中以乙醚-二氯甲烷3:1(V/V)提取。固定相为YWG C_(18)H_(37),流动相为MeOH-0.02mol/L HAc(pH 5.5)65:35(V/V)、卡马西平(CZ)作内标,UV 280nm检测。线性范围0.24~22.8μg/ml,γ=0.999 9。最低检测浓度为60ng/ml。提取回收率为95.83%~97.58%。方法回收率为100.33%~106.46%。天内及天间精密度(GV)各为0.55%~1.11%及1.40%~2.91%。

The synthesis routes for Diclofenac Sodium were recieved, and the title compound was also prepared in a more convenient way.

本文概述了新型解热镇痛药双氯灭痛的合成路线,对其中一步直接缩合法合成该化合物进行了研究,从而提供了一条较有工业化前景的合成路线。

Diclofenac Sodium has been synthesized from o-chlorophenylacetic acidderivative and 2,6-dichlorophenylamine under cuprous iodide as catalyst.we have studied the influential factors on the yield.

双氯灭痛可由邻氯苯乙酸衍生物和2,6—二氯苯胺合成而得。本文研究了影响产率的多种因素。

 
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