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     The Effects of Zn~2+ and Sr~2+ in Seawater on the Hatchability and Metamorphosis Rate of Artemia saline
     海水中Zn~(2+)(锌离子)和Sr~(2+)(锶离子)对卤虫卵孵化率和幼体变态率的影响
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     A study on new protective coating-Zn-Ni alloy electroplating process
     新防护性镀层Zn-Ni(锌/镍)合金工艺研究
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     mg/kg of zinc in basal diet.
     B组:基础日粮+Zn 40 mg/(d.头)(锌含量48.12 mg/kg);
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     Five groups diets were as follows: A group diet was control group with zinc level of 39.69 mg/kg, B, C, D, E group diets had zinc level of 48.12 mg/kg, 53.83 mg/kg, 59.55 mg/kg, 65.26 mg/kg respectively.
     A组:对照组,饲喂锌含量水平39.69mg/kg的基础日粮; B组:基础日粮+40mg Zn/日·头(锌含量水平48.12mg/kg);
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     mg and 100? mg/(day·ram)(levels of zinc were 48.12?mg/kg,53.83?mg/kg,59.55?mg/kg and 27?mg/kg),respectively.
     E组:基础日粮+Zn 100 mg/(d.头)(锌含量65.26 mg/kg)。
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     ZINC
    
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     The Comparison of the Freezing Point of Zinc
     凝固点的比较
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     Zinc electrode(4)
     电极(4)
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     Zinc electrode(6)
     电极(6)
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  (zn
The circulant digraphDCn(S) is a directed graph with vertex setZn and arc set {(i,i+s): i ∈ Zn, s ∈ S}.
      
The precursor was proved to be [Zn5(OH)6(CO3)2] by TG-DTG-DTA and IR analysis.
      
Electrically conductive composites were prepared via the chemical oxidative polymerization of the pyrrole monomer in polystyrene (PS) and zinc neutralized sulfonated polystyrene (Zn-SPS) films under supercritical carbon dioxide (SC-CO2) conditions.
      
The percolation thresholds of PS/PPy and Zn-SPS/PPy composites were 6.2% and 2.7% of the volume fraction of PPy, respectively, much lower than the theoretically predicted value of 16%.
      
The reversible capacity of SnO2 · Zn2SnO4 is 758 mA · h/g in the first cycle and the charge capacity is 455 mA · h/g in the tenth cycle.
      
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p-Nitro-acetophenone was prepared by diazotizing p-amino-acetophenone in fluoroboric acid solution and replacing the diazonium fluoroborate group by the nitro group in presence of finely divided copper as catalyst. Yield 55-60%; m.p. 76-78℃. Recrystallization from alcohol gave a product of m.p. 80℃.

從乙醯苯胺、醋酸酐與氯化鋅作用,經水解後製得對胺基苯乙酮。在氟硼酸水溶液中重氮化之,再在亞硝酸鈉的水溶液中以銅粉為觸媒,將此重氮團置換成爲硝基,即得對硝基苯乙酮。

The effects of copper and zinc ionsupon the precipitation of barium sul-phate have been noted for a long time.However,the results published wereeither not systematic(3,4b,5,6)or obtained under conditions apart fromusual analytical practice(7,8).Thus,it seems necessary to investigate thissubject in more detail by the usual methods of determination.The presentcommunication reports(a)the effect of various amounts of cupric and zincions and(b)the influence of different acidities during precipitation in thepresence...

The effects of copper and zinc ionsupon the precipitation of barium sul-phate have been noted for a long time.However,the results published wereeither not systematic(3,4b,5,6)or obtained under conditions apart fromusual analytical practice(7,8).Thus,it seems necessary to investigate thissubject in more detail by the usual methods of determination.The presentcommunication reports(a)the effect of various amounts of cupric and zincions and(b)the influence of different acidities during precipitation in thepresence and absence of zinc ions.It is found that the interference of copper in the determination of sulphuras barium sulphate up to a ratio of 20:1 for Cu:S is negligible.The deviationsof the results obtained from theoretical values are all within ±2‰(see Table1),and do not show any regularity with the amount of copper added.The presence of zinc ions alone gives satisfactory results(slightly lowerthan theoretical values).As the amount of zinc ions in solution increases,thedeviations become somewhat wider(Table 2).The low results are presumedto be due to(1)the formation of soluble zinc-sulphate complex,which holdsa part of sulphate in solution,and/or(2)diverse ion effect.In the presenceof zinc ions,introducing hydrochloric acid up to 0.1 N before precipitationcauses essentially the same errors as if hydrochloric acid were absent(cf.Tables2 and 3),while at and beyond 0.2 N positive errors are obtained.A spectrographic examination of the precipitates reveals that zinc doescoprecipitate with barium sulphate,though only to a slight extent.The amountof zinc coprecipitated decreases with the increase of the acidity of the solutionfrom which the precipitate is thrown down.

本文报告铜及离子对于硫酸钡定硫的影响,找出了铜的影响几近于零,的影响亦微。离子能与硫酸钡共同沉淀。

Aureomycin (Ⅰ) on reduction with zinc-acetic acid gives desdimethylaminoaureomycin (Ⅱ) under mild conditions and desdimethylaminodesoxyaureomycin (Ⅲ) under more drastic conditions. Ⅱ can be converted into Ⅲ by further reduction. Treatment of Ⅰ, Ⅱ or Ⅲ with concentrated hydrochloric acid or methanolic HCl produces anhydroaureomycin (Ⅳ), desdimethylaminoanhydroaureomycin (Ⅴ) or desdimethylaminodes- oxyanhydroaureomycin (Ⅵ) respectively. Compound (Ⅴ) can be obtained from Ⅳ by hydrogenolysis, and, similarly, Ⅵ...

Aureomycin (Ⅰ) on reduction with zinc-acetic acid gives desdimethylaminoaureomycin (Ⅱ) under mild conditions and desdimethylaminodesoxyaureomycin (Ⅲ) under more drastic conditions. Ⅱ can be converted into Ⅲ by further reduction. Treatment of Ⅰ, Ⅱ or Ⅲ with concentrated hydrochloric acid or methanolic HCl produces anhydroaureomycin (Ⅳ), desdimethylaminoanhydroaureomycin (Ⅴ) or desdimethylaminodes- oxyanhydroaureomycin (Ⅵ) respectively. Compound (Ⅴ) can be obtained from Ⅳ by hydrogenolysis, and, similarly, Ⅵ from either IV or V. All the above compounds, (Ⅰ), (Ⅱ), (Ⅲ), (Ⅳ), (Ⅴ) and (Ⅵ), when subjected to zinc dust distillation, form naphthacene. A comparison of the ultra-violet absorption spectra of Ⅰ, Ⅱ, Ⅲ, Ⅳ, Ⅴ and Ⅵ affords a supplementary evidence for the location of the angular-OH group in the structure of aureomycin.

金黴素(I)在冰醋酸與甲醇溶液中,用鋅粉氫解,在温和條件下,產生脫二甲胺金黴素(II);較劇烈條件下,則生成脫二甲胺脫羥金黴素(III)。III從II經鋅粉醋酸氫解得到。 I,II,III分別與濃鹽酸或甲醇鹽酸處理相應地得到脫水金黴素(IV),脫二甲胺脫水金黴素(V)及脫二甲胺脫羥脫水金黴素(VI)。脫水金黴素(IV)經鋅粉醋酸氫解亦產生V與VI。VI亦可從V製成。 I,II,III,IV,V或VI和鋅粉共同蒸餾,皆得到并四苯。 從紫外吸收光譜測定,對金黴素結構中二甲胺基及角羥基的位置有補充的說明。

 
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